山核桃油的提取工艺及其特性研究
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    摘要:

    对乙醚浸提法提取山核桃油的工艺条件进行了试验。结果表明:液料比大于4 mL/g、提取温度为55~65℃、提取时间2.5 h,山核桃油的提取率较高。在单因素试验的基础上用正交试验得出优化工艺条件为:液料比为5 mL/g、温度65℃、时间2.5 h,在该条件下山核桃油的提取率为98.17%。油脂的理化指标为:碘价92.20 g/100 g、折光指数n201.471 0、相对密度d200.905 6、酸价0.750 mg/g。采用气相色谱-质谱分析仪对油脂的脂肪酸组成及含量进行了测定,结果表明,不饱和脂肪酸质量分数为91.51%,其中油酸和亚油酸质量分数为

    Abstract:

    91.13%。 The ether extracting technology of carya kernel oil was experimentally studied in this work. The result showed that a high extraction rate could be achieved when the ratio of solution/material was higher than 4 mL/g,operating temperatures ranged from 55 to 65℃ and the duration of extraction was 2.5 h. On basis of single factor experiment,the orthogonal trial was used in optimization of technological parameters,the optimum technological condition was 5 mL/g,2.5 h and 65℃,under which the extraction rate could be high as 98.17%. Physicochemical properties of the oil are as follows: the iodine value is 92.20 g/100 g; the refractive index n201.471 0, density d200.905 6 and the acid value 750 mg/g. The unsaturated fatty acid in the oil was 91.51%,the oleic acid and the linoleic acid was both 91.13% determined by the gas chromatography-mass spectroscopy(GC-MS).

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周明亮,王鸿飞,赵丹.山核桃油的提取工艺及其特性研究[J].农业机械学报,2007,38(3):95-98.

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