豆粕品质近红外定量分析实验室模型在线应用
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国家重点研发计划项目(2017YFE0115400、2016YFE0204600)和现代农业(奶牛)产业技术体系建设专项资金项目(CARS-36)


Online Application of Soybean Meal NIRS Quantitative Analysis Model from Laboratory to Factory
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    摘要:

    为探究豆粕近红外定量分析模型从实验室到工厂在线应用转移的可行性,以全国采集的117个豆粕样品为研究对象,利用偏最小二乘法在实验室建立了豆粕含水率、粗蛋白质量分数的近红外定量分析模型,继而将此模型转移到饲料生产企业进行在线应用。研究结果显示:建立的实验室近红外模型可实现豆粕含水率、粗蛋白质量分数的快速预测,其中,含水率和粗蛋白质量分数的验证集决定系数R2P分别为0.83和0.86,相对分析误差分别为2.40和2.55,模型效果良好;采用模型校正、样品扩充两种不同方法,将实验室模型转移到饲料生产企业进行在线应用,含水率和粗蛋白质量分数的预测值与实际测量值之间具有很好的吻合性,可以达到在线分析的要求。

    Abstract:

    Aiming to explore the feasibility of the online nearinfrared quantitative analysis model of soybean meal from laboratory to factory transfer and application. Totally 117 soybean meal samples were collected nationwide and used, the nearinfrared quantitative analysis models of moisture and crude protein were established in the laboratory by partial least squares method, two kinds of nearinfrared online equipment installation methods were used in feed production enterprises. The laboratory models of nearinfrared quantitative analysis of soybean meal quality were transferred to feed production enterprises for online application by two different methods. The results showed that laboratory model can rapidly predict the content of moisture and crude protein in soybean meal (RSD was below 10%), R2P of moisture and crude protein were 0.83 and 0.86, RPD value of moisture and crude protein were 2.40 and 2.55, which meant that the model effect was fine; laboratory models were transferred to feed production enterprises for online analysis by different methods such as model correction and sample expansion, the deviation between the predicted value and the measured value was small and stable. The requirement for online detection can be achieved.

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杨增玲,杨钦楷,沈广辉,梅佳琪,黄圆萍,韩鲁佳.豆粕品质近红外定量分析实验室模型在线应用[J].农业机械学报,2019,50(8):358-363,371.

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  • 收稿日期:2019-01-28
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  • 在线发布日期: 2019-08-10
  • 出版日期: 2019-08-10